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Continuous Flow Coupling and Decarboxylation Reactions Promoted by Copper Tubing

Zhang, Yun and Mainolfi, Nello and Patel, Sejal and Timothy, Jamison/F (2011) Continuous Flow Coupling and Decarboxylation Reactions Promoted by Copper Tubing. Journal of Organic Letters, 13 (2). pp. 280-283. ISSN 1523-7060

Abstract

A convenient and efficient flow method for Ullmann condensations, Sonogashira couplings, and decarboxylation reactions using a commercially available copper tube flow reactor (CTFR) is described. The heated CTFR effects these transformations without added metals (e.g., Pd), ligands, or reagents, and in greater than 90% yield in most cases examined.

Item Type: Article
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Additional Information: Archiving not formally supported
Keywords: flow, Ullmann condensation, Sonogashira coupling, decarboxylation, copper tube reactor
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Date Deposited: 13 Oct 2015 13:15
Last Modified: 13 Oct 2015 13:15
URI: https://oak.novartis.com/id/eprint/3948

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