Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state.
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Baltus, Christine, Press, Neil, Antonijevic, Milan, Tizzard, Graham, Coles, Simon and Spencer, John (2012) Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state. Tetrahedron, 68 (45). pp. 9272-9277. ISSN 0040-4020
Official URL: http://www.sciencedirect.com/science/article/pii/S...
Abstract
A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki-Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4'-methylbiphenyl-4-yl)acetamide with Z'=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.
| Item Type: | Article |
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| Additional Information: | CASE collaboration |
| Keywords: | Cross coupling, microwaves, biphenyl amides, hydrogen bonds, Z', X-ray crystallography. |
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| Date Deposited: | 13 Oct 2015 13:14 |
| Last Modified: | 13 Oct 2015 13:14 |
| URI: | https://oak.novartis.com/id/eprint/7015 |