Browse views: by Year, by Function, by GLF, by Subfunction, by Conference, by Journal

Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state.

Baltus, Christine and Press, Neil and Antonijevic, Milan and Tizzard, Graham and Coles, Simon and Spencer, John (2012) Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state. Tetrahedron, 68 (45). pp. 9272-9277. ISSN 0040-4020

Abstract

A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki-Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4'-methylbiphenyl-4-yl)acetamide with Z'=6 and hydrogen-bonding networks of the type N–H…O in the unit cell.

Item Type: Article
Related URLs:
Additional Information: CASE collaboration
Keywords: Cross coupling, microwaves, biphenyl amides, hydrogen bonds, Z', X-ray crystallography.
Related URLs:
Date Deposited: 13 Oct 2015 13:14
Last Modified: 13 Oct 2015 13:14
URI: https://oak.novartis.com/id/eprint/7015

Search

Email Alerts

Register with OAK to receive email alerts for saved searches.